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The Chemical Educator

ISSN: 1430-4171 (electronic version)

Table of Contents

Abstract Volume 8 Issue 3 (2003) pp 199-200

A Heated Cuvette Holder for Fiber-Optic Ultraviolet–Visible Spectrophotometers

Gary W. Breton,* Dwight Kinzer, and John H. Shugart

Berry College, P.O. Box 495016, Mount Berry, GA 30149–5016, gbreton@berry.edu
Received February 10, 2003. Accepted March 30, 2003

Published online: 25 April 2003

Abstract. The design and construction of a novel heated cuvette holder for fiber optic UV–vis spectrophotometers is described. The cuvette holder is especially useful for determining the kinetics of reactions at temperatures greater than 100 °C. Kinetics for the Diels–Alder reaction of tetraphenylcyclopentadienone with diphenylacetylene are investigated at several temperatures as an illustration of the benefits of the new system.

Key Words:  Laboratories and Demonstrations; physical chemistry; instrumental analysis; kinetics

(*) Corresponding author. (E-mail: gbreton@berry.edu)

Article in PDF format (469 K B) HTML format

Supporting Materials:

Complete schematic drawings for the heated cuvette holder, additional pictures of the cuvette holder, and experimental details for the Diels-Alder reaction are included in a Zip file (766 KB). 10.1007/s00897030684a

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Issue date: June 1, 2003

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