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The Chemical Educator

ISSN: 1430-4171 (electronic version)

Table of Contents

Abstract Volume 29 (2024) pp 128-131

Green Chemistry Technology/Synthesis of Silver Nanoparticles onto Working Electrode Utilizing Electrochemistry to Detect Phenol

Nicholas Shonkwiler, Bryce Werts, and Suzanne K. Lunsford*

Department of Chemistry, Wright State University, 3640 Colonel Glenn Highway, Dayton, Ohio 45435, Suzanne.Lunsford@wright.edu

Received April 11, 2024. Accepted June 10, 2024.

Published: 3 December 2024

Abstract. Our inquiry based lab experiment involved optimizing the ideal working electrode with a novel material such as nanoparticles to detect phenol using CV (cyclic voltammetry) and DPV (differential pulse voltammetry). Students were required to learn electrochemical instrumentation and determine how to enhance the electrode response with synthesized silver nanoparticles (AgNPs) to detect phenol in water at various pH values. Our students in the undergraduate chemistry course have found the electrochemistry instrumentation with hands-on experiences rewarding to understand important environmental issues. This lab educated our students on real-world analysis/detection of common hazardous pollutants such as phenol by differential pulse voltammetry (DPV) while integrating synthesis of nanoparticles (silver nanoparticles) deposited onto a working electrode.

Key Words: Laboratories and Demonstrations; analytical chemistry;

(*) Corresponding author. (E-mail: Suzanne.Lunsford@wright.edu)

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